Spyros Mourtas, Dimitrios Gatos, Manolis Karavoltsos, Christina Katakalou, and Kleomenis Barlos

Tetrahedron Letters 2002; 43(18): 3419-3421. https://doi.org/10.1016/S0040-4039(02)00461-6

Abstract:
Mercapto acids were attached through their thiol group onto 2-chlorotrityl (Clt)-, trityl (Trt)-, 4-methyltrityl (Mtt)-, 4-methoxytrityl (Mmt)-, and 4,4'-dimethoxytrityl (Dmt)-resins. The new resins were used in the solid-phase synthesis of small mercaptoacylamino alcs. Cleavage from the resins was performed by treatment with trifluoroacetic acid (TFA) solutions in dichloromethane (DCM) using triethylsilane (TES) as scavenger.